MW Photo Group 2011
  • UCLM – Organic Microwave Chemistry

  • Our broader area of expertise include Microwave Chemistry, Heterocyclic Chemistry, Computational Chemistry and more recently we have expanded into Nano Chemistry (nanotubes, graphene, etc..) NMR Foods Analysis, and Chemistry-on-flow.

    Contact purposes: Prof. Antonio de la Hoz Ayuso

    Organic Chemistry Professor
    Avda. Camilo José Cela, 10 – 13071 Ciudad Real
    Web: www.umsoc.com / www.uclm.es Tfno. 926295411

MW Photo Group 2011

Review on the use of NMR spectroscopy in flow chemistry

This review show the recent advances in the use of flow chemistry with in-line and on-line analysis by NMR. It cover from the use macro- and, microreactors, standard and custom made NMR probes involving microcoils, high resolution and benchtop NMR instruments and the use of DOE and automatic reaction monitoring and automatization. Selected applications have been collected … Continue reading

Book chapter on flow Chemistry

A new book chapter on the use of non-conventional techniques in sustainable chematry under flow conditions has been published by our group. The chapter it is included in the book Sustainable Flow Chemistry – Chapter 9. Methods and Applications.  Edited by L. Vaccaro and published by Wiley-VCH.

New review on computational calculations and microwave irradaition

This review, published in Chem. Soc. Rev., provides an overview of the use of Computational Chemistry in MAOS to provide a theoretical understanding of the factors that can be used to explain the improvements in MAOS and how computational calculations can be used as a predictive tool.

Publicación convocatoria Ayudas para la formación de profesorado Universitario FPU-2016

Se han convocado 850 contratos predoctorales de cuatro años para la realización de Tesis doctorales en Universidades y centros de investigación. Requisitos: Estar matriculados en un programa de doctorado en una universidad española en el curso 2016-2017. Alternativamente, los solicitantes podrán acreditar que en el momento de presentación de las solicitudes se encuentran en posesión del título … Continue reading

Convocatoria de contratos predoctorales para la formación de personal investigador en el marco del Plan Propio de Investigación UCLM

La UCLM ha convocado hasta 30 contratos predoctorales para realizar tareas de investigación con las siguientes características: Dotación: 23.000 € anuales durante los tres primeros años. Cuarta anualidad (23000 €), si se ha defendido la Tesis podrá utilizarse como estancia postdoctoral (25000 €). Requisitos: Estar matriculados en un programa de doctorado de la UCLM. Alternativamente … Continue reading

New book chapter on Microwaves in Green Chemistry

Since the first publications on the use of microwave irradiation in synthetic chemistry, it was clear that this methodology would have a marked influence in all areas of this discipline. Reduction of reaction times, improved yields, modifications of selectivities, increased product purities and simplification of work-up procedures were described and, in most cases, these conditions … Continue reading

Call for a PhD position in the University of Turin

An open call for a PhD position in the University of Turin (3 years grant) under the supervision of Prof. Giancarlo Cravotto will be soon available, candidates have to select one of the two following projects: 1) Innovative technologies for the recovery, adsorption or degradation of pharmaceuticals and other persistent organic pollutants from industrial or urban … Continue reading

New paper on molecular recognition: triazine-carbon nanotubes with Flavin

Carbon nanotubes, both single-walled and multi-walled, have been functionalised with 1,3,5-triazines and p-tolyl chains by aryl radical addition under microwave irradiation and the derivatives have been fully characterised. Artificial receptors in catalytic processes could be designed through specific control of the interaction between functionalised carbon nanotubes and riboflavin.

Preparation and properties of Triazine based Streptocyanines

A new series of bistriazine-based streptocyanines has been selectively prepared. 1D- and 2D-DNMR spectroscopy and computational calculations have shown the presence of a Cl … H bond. UV–vis and fluorescence spectroscopy show that streptocyanine-based bistriazines are violet-blue emitters and large Stokes shifts of more than 6000 cm−1 were observed. The title compounds showed interesting properties which … Continue reading

SMALL-VOLUME NMR spectroscopy

NMR analysis of mass-limited samples remains a major challenge, which has triggered the development of expensive superconducting ultra-high field magnets, as well as of more expensive and technologically demanding solutions as cryoprobes and hyperpolarization schemes. Mass-limited samples could also benefit from the use of miniaturized coils, since the amplitude of the NMR signal is optimal … Continue reading